ࡱ> [ JbjbjXX 3:ji:jiBdd   8B < b2"Zt#t#t#t#O$"q$ }$nbpbpbpbpbpbpb$!fhtb$O$O$$$bt#t#b,,,$t#t#nb,$nb,,>4@t#Pz+%?Zbb0b@Ki&4Ki(@@KiY$$,$$$$$bb)$$$b$$$$Ki$$$$$$$$$dX : DALE K. HENSLEY Curriculum Vitae Controlled Synthesis Engineer and Master Technician Nanofabrication Research Laboratory 91 /staff-profile/dale-k-hensley Summary Research Synopsis (2001 present) Participated in several interdisciplinary research teams in the following projects:Neuronal interfaces, Cell mimic, Membrane mimic, Digital Electrostatically focused e-beam Array direct-write Lithography (DEAL), Intracell, Maximus, Thin-film transistor arrays, F-extraction, Nanostructured Gene Delivery Arrays and ORNL-6, Technology Innovation Program (TIP) - Rapid, Fieldable Viral Diagnostics, also participate in CNMS User projects. Characterization of samples with a wide range of chemistries and morphologies from bulk to nano features and non-conducting samples by utilization of scanning electron microscopies with energy-dispersive x-ray spectroscopy. Controlled Synthesis Engineer in the Nanofabrication Research Laboratory group (NRL), Nanomaterials Synthesis/Nanofabrication section, Center for Nanophase Materials Sciences (CNMS) Division, Physical Sciences Directorate, 91 (ORNL). Expertise in carbon materials synthesis, physical vapor deposition of metals, and materials characterization, vital for understanding nanoscale materials. Participates with multi-disciplinary teams on research projects, providing synthesis, fabrication, and characterization expertise, with over 200 peer-reviewed co-authored publications. Master Technician, providing operational and technician support to achieve the goal of publishing scientific papers. Responsibilities include tool(s) ownership/training/support, chemical/waste management, general lab operations, user training, and lab space manager. Technical Support since August 1983, for several research areas and three user facilities, the Oak Ridge Electron Linear Accelerator (ORELA), the Surface Modification and Characterization Research Center (SMAC), and CNMS at ORNL.Was involved in the beginning phase of the CNMS where the initial focus was being part of the team to bring the NRL online. Presently supports nanofabrication research in the NRL. Committed to assisting scientific innovation by providing technical support, operational excellence in safety and equipment uptime, mentoring researchers by trainings and advising , and community/education outreach by giving tours at CNMS and the ORNL traveling science fair trailers. Recognized for contributing to the development of a custom-built plasma enhanced chemical vapor deposition (PECVD) system for synthesis of carbon based nanotechnology. Carbon nano spikes (CNS) act as room temperature/pressure conduits for electrons to promote reaction with other chemicals, by creating high localized electric fields. In an electrolytic cell, an electrode composed of CNS can enable catalytic reduction of common chemicals to high-value products (nitrogen to ammonia, carbon dioxide to ethanol and heavier carbon chains). Also, CNS is a form of graphene with many edge planes; on wires, they makeCNS-modified nanoelectrodes. CNS have enhanced surface roughness and surface oxide concentration, increasing their sensitivity to dopamine and other neurochemicals. Arrays of Vertically Aligned Carbon Nano-fibers (VACNF) may be implemented for massively parallel DNA delivery. By adsorbing or covalently linking DNA to nanofiber arrays, cells are providednew genetic material simply by impaling them upon the DNA-modified nanofiber array. VACNF have also been used as electron emitters.VACNF are deterministically synthesized by PECVD, and compatible with microfabrication processing, They have subcellular dimensions, making them suitable for biochip cell interface. They are made of carbon which is a good material for electrochemical probes. They have rich side-wall chemistry for chemical derivatization and immobilization of macromolecules. Finally, the location of VACNF is lithographically defined, and individually addressable nano-electrodes can be manufactured. Notable recent awards related to CNS: ORNL Innovation Awards for three U.S. patents (2023, 2019, 2017) ORNL Innovation Award for licensing agreements with Prometheus Fuels Inc. and Reactwell LLC (2021) Federal Laboratory Consortium National Technology Transfer Impact Award - for A Catalyst to Produce Ethanol and Reduce reliance on Fossil Fuels. (2020) R&D 100 award - for Voltanol: Electrochemical Conversion of Carbon Dioxide to Ethanol. (2019) Excellence in Technology Transfer Award, Southeast Region, from the Federal Laboratory Consortium for Licensing of ORNL Electrochemical Catalyst for Conversion of CO2 to Ethanol. (2019) CNMS Outstanding Scientific or Technical Contribution Award for Discovery of a novel electrochemical reaction in which Carbon Dioxide is converted directly into Ethanol. (2017) Professional Experience 1983 present 91, Oak Ridge, Tennessee Controlled Synthesis Engineer, Center for Nanophase Materials Sciences (CNMS) Division, ORNL (11/05present) Controlled Synthesis Research Associate, Molecular-Scale Engineering and Nanoscale Technologies group, Condensed Matter Sciences Division, ORNL. (12/200111/2005) Principal Technologist, Surface Modification and Characterization Research Center (SMAC), Solid State Division, ORNL (3/199112/2001) Engineering Technologist, Oak Ridge Electron Linear Accelerator (ORELA), ORNL (8/19833/1991) Electronic Technician, CBS, Carrollton, Georgia (4/1983 8/1983) Education  1983 Fountainhead College of Technology, Knoxville, Tennessee Associate Electronic Technology Additional Training: Successful completion of courses resulted in Certificates of Training from the American Vacuum Society: Plasma Enhanced Chemical Vapor Deposition, Plasma Etching and Reactive Ion Etching, Basics of Radio Frequency, Surface Preparation for Thin-Film Deposition, Thin Film Deposition by Evaporation, Operation/Maintenance and Leak Detection of Vacuum Systems, Scanning Electron Microscopy and X-ray Microanalysis. Energy Dispersive X-ray Micro Analysis from EDAX/Ametek. Laboratory Operations Supervisor Academy, a Battelle program that helps front-line leaders build a culture that supports the HYPERLINK "https://sbms.ornl.gov/sbms/safeconduct.pdf" Safe Conduct of Research. Professional Organizations Symposium of North Eastern Accelerator Personnel (19912000) American Vacuum Society Science and Technology of Materials, Interfaces, and Processing (20012013) Microscopy Society of America 2013 present Electron, Ion, and Photon Beam Technology and Nanofabrication (2015 2019) Patents and Invention Disclosures  YEARPATENTSTITLEINVENTORS2017US 9,637,828Electrochemical Method for Synthesizing Metal-Containing Particles and Other ObjectsAdam Justin Rondinone, Ilia N Ivanov, Sean Campbell Smith, Chengdu Liang, Dale K Hensley, Ji-Won Moon, Tommy Joe Phelps2019US 10,450,663 HYPERLINK "https://patents.google.com/patent/US10450663B2/en" Electrochemical catalyst for conversion of nitrogen gas to ammoniaAdam J Rondinone, Peter V Bonnesen, Dale K Hensley, Rui Peng, Yang Song2022US 11,519,087Alloy Based Electrochemical Catalyst for Conversion of Carbon Dioxide to HydrocarbonsAdam J Rondinone, Dale K Hensley, Seonah JinYEARDISCLOSURESTITLEINVENTORS2013ID201303002Nanotextured, Non-Plating Electrode for Low Temperature Electrochemical Nanoparticle Synthesis and Other Particulate Electrochemical ReactionsAdam Justin Rondinone, Ilia N Ivanov, Sean Campbell Smith, Chengdu Liang, Dale K Hensley, Ji-Won Moon, Tommy Joe Phelps2013ID13-076 NCSAirbrushed Nickel Nanoparticles for Large-Area Growth of Vertically Aligned Carbon Nanofibers on Metal (Al, Cu, Ti) SurfacesAnatoli Melechko, Ryan Pearce, Justin Railsback, Bryan Anderson, Mehmet Sarac, Joseph Tracy, Dale Hensley, Tim Mcknight2014ID 201403439Electrochemical Catalyst for Conversion of CO2 to EthanolAdam J Rondinone, Peter V Bonnesen, Dale K Hensley, Rui Peng, Yang Song2016ID201603762Electrocatalytic Nitrogen Fixation for the Synthesis of Ammonia at Room Temperature and PressureDale K. Hensley, Adam J. Rondinone, Yang Song2017ID201703862A Wireless Hydrogen Fluoride DosimeterBrian B. Anderson, Dale K. Hensley, James Humphries, Matthew Lassiter, Andrew Miskowiec Selected Publications Sulfur functionalized biocarbon sorbents for low-concentration mercury isolation Douglas Austin, Kousar Jahan, Xu Feng, Jared Carney, Dale K Hensley, Jihua Chen, Brianna E Altidor, Zhiyong Guo, Elizabeth Michaelis, Mariana K Kebaso, Yanfeng Yue Dalton Transactions (2024) Carbon nanospikes have improved sensitivity and antifouling properties for adenosine, hydrogen peroxide, and histamine He Zhao, Kailash Shrestha, Dale K Hensley, B Jill Venton Analytical and Bioanalytical Chemistry (2023) Carbon nanospike coated nanoelectrodes for measurements of neurotransmitters Q Cao, Z Shao, D Hensley, BJ Venton Faraday Discussions (2022) Polymer, additives, and processing effects on N95 filter performance GS Larsen, Y Cheng, LL Daemen, TN Lamichhane, DK Hensley, K Hong ACS Applied Polymer Materials (2021) Work function measurements of clean and modified carbon nanospikes AP Baddorf, AJ Rondinone, DK Hensley Carbon (2020) DatabaseAuthor IDDocumentsCitationsh-IndexOtherSCOPUS35499268500170461639Field-weighted citation impact 1.52Google ScholarBswnLAEAAAAJ&hl=en221560039Research Gate208479339Research-interest score 2298 Awards and Recognitions 2020 National Technology Transfer Impact Award, Federal Laboratories Consortium For A Catalyst to Produce Ethanol and Reduce reliance on Fossil Fuels 2019 R&D 100 Award, R&D World For the development of Voltanol: Electrochemical Conversion of Carbon Dioxide to Ethanol. 2019 Southeast Region Excellence in Technology Transfer Award, Federal Laboratory Consortium Licensing of ORNL Electrochemical Catalyst for Conversion of CO2 to Ethanol. 2017 Grand Prize, International Conference on Electron, Ion, and Photon Beam Technology and Nanofabrication, Micrograph Competition 2016 First Prize, Class 5, International Metallographic Society, Micrograph Competition 2016 First Prize, Class 4, International Metallographic Society, Micrograph Competition 2016 Third Prize, Class 4, International Metallographic Society, Micrograph Competition 2014 First Prize, Microscopy Society of America Microscopy & Microanalysis, Micrograph Competition 2011 Certificate of Recognition: Mentor for Teachers as Researchers, Siemens Foundation Preparing Science & Technology Leaders for the future in Microanalysis. 1998 Technical Achievement Award, Lockheed Martin For developing a novel time-shared, foreline and roughing, vacuum system for the Surface Modification and Characterization Research Center. Organizational Recognitions 2020 Award for Excellence in Mission Support, UT-Battelle For multiple mission-critical accomplishments in the stripper foil R&D. 2016 Award for Excellence in Mission Support, UT-Battelle For the successful execution of a complex project to improve the synthesis, production, and performance of the diamondstripper foils for the operation of the Spallation Neutron Source. 2008 Team Award for Technical Support, UT-Battelle For successful operation of the Nanofabrication Research Laboratory and the growth of a vibrant user community. ORNL Recognitions 2023 Physical Sciences Directorate Technician Core Values Award For Service to the Community 2023 Innovation Award For U.S. Patent No. 11,519,087 2021 Innovation Award For Licenses with Prometheus Fuels Inc. and Reactwell LLC 2020 Significant Performance Award 2020 Innovation Award For a License, a Patent and a National FLC award 2019 Technology Commercialization Award For a successful license to Reactwell 2018 Art of Science contest finalists Two images were chosen for the top 20 2018 Technology Commercialization Award For a successful license to Reactwell 2018 Technology Commercialization Award For a successful license to Solsys Energy 2017 CNMS Outstanding Scientific or Technical Contribution Award For Discovery of a novel electrochemical reaction in which Carbon Dioxide is converted directly into Ethanol with both high yield and High selectivity 2017 Top ORNL science news stories For 2016, the news release and video about an ORNL-developed nano-spike catalyst that converts carbon dioxide into ethanol received substantial media attention, in large part thanks to a viral Popular Mechanics article that was cited as the outlet's most popular story of the year 2016 Supplemental Performance Award For coauthoring 14 published papers in FY16 2015 Master Technician Top of ORNLs Technical Support Ladder 2014 Supplemental Performance Award For sharing nano science technology to the general and science attentive public effectively through tours and outreach 2012 Supplemental Performance Award For contributing to the installation and startup of the Helium Ion Microscope 2011 Significant Event Award For important contributions in the installations and start-up ofAARA- procured advanced microscopes for Electron Microscopy with Soft-Material Emphasis in the CNMS and provided training to users of these microscopes Selected Media Coverage HYPERLINK "/news/nano-spike-catalysts-convert-carbon-dioxide-directly-ethanol"/news/nano-spike-catalysts-convert-carbon-dioxide-directly-ethanol October 12, 2016 HYPERLINK "https://www.greencarcongress.com/2016/10/20161013-ornl.html"https://www.greencarcongress.com/2016/10/20161013-ornl.html October 13, 2026 HYPERLINK "https://www.popularmechanics.com/science/green-tech/a23417/convert-co2-into-ethanol/"https://www.popularmechanics.com/science/green-tech/a23417/convert-co2-into-ethanol/ October 17, 2016 HYPERLINK "https://www.cbsnews.com/minnesota/news/scientists-turn-co2-into-ethanol/"https://www.cbsnews.com/minnesota/news/scientists-turn-co2-into-ethanol/ October 19, 2016 HYPERLINK "https://time.com/4536708/carbon-dioxide-ethanol/"https://time.com/4536708/carbon-dioxide-ethanol/ October 19, 2016 HYPERLINK "https://www.youtube.com/watch?v=grGpTa9zxQM"https://www.youtube.com/watch?v=grGpTa9zxQM October 21, 2016 HYPERLINK "https://insights.globalspec.com/article/3472/nanospike-catalysts-convert-co2-into-ethanol"https://insights.globalspec.com/article/3472/nanospike-catalysts-convert-co2-into-ethanol October 26, 2016 HYPERLINK "https://oakridgetoday.com/tag/carbon-dioxide-to-ethanol-conversion/"https://oakridgetoday.com/tag/carbon-dioxide-to-ethanol-conversion/ January 18, 2017 HYPERLINK "/blog/ornl-reporter/nano-spike-catalysts-convert-co2-directly-ethanol-production-0"/blog/ornl-reporter/nano-spike-catalysts-convert-co2-directly-ethanol-production-0 March 15, 2017 HYPERLINK "/news/novel-reaction-could-spark-alternate-approach-ammonia-production"/news/novel-reaction-could-spark-alternate-approach-ammonia-production May 2, 2018 HYPERLINK "https://www.linkedin.com/pulse/flc-2019-southeast-excellence-technology-transfer-ornl-cochran?trk=read_related_article-card_title"https://www.linkedin.com/pulse/flc-2019-southeast-excellence-technology-transfer-ornl-cochran?trk=read_related_article-card_title October 18, 2019 HYPERLINK "/news/reactwell-licenses-ornl-catalyst-energy-conversion-applications"/news/reactwell-licenses-ornl-catalyst-energy-conversion-applications March 1, 2019 HYPERLINK "https://federallabs.org/flc-highlights/awards/licensing-of-ornl-electrochemical-catalyst-for-conversion-of-co2-to-ethanol-267a59d7f591b0c2d14333ae018162b9"https://federallabs.org/flc-highlights/awards/licensing-of-ornl-electrochemical-catalyst-for-conversion-of-co2-to-ethanol-267a59d7f591b0c2d14333ae018162b9 October 16, 2019 HYPERLINK "https://www.rdworldonline.com/rd-100-2019-winner/voltanol-electrochemical-conversion-of-carbon-dioxide-to-ethanol/"https://www.rdworldonline.com/rd-100-2019-winner/voltanol-electrochemical-conversion-of-carbon-dioxide-to-ethanol/ December 5, 2019 HYPERLINK "/news/ornl-receives-four-2020-flc-technology-transfer-awards"/news/ornl-receives-four-2020-flc-technology-transfer-awards March 4, 2020 HYPERLINK "/news/2019-rd-100-winner-voltanol-electrochemical-conversion-carbon-dioxide-ethanol"/news/2019-rd-100-winner-voltanol-electrochemical-conversion-carbon-dioxide-ethanol March 23, 2020 HYPERLINK "/news/tech-transfer-fueling-retooling"/news/tech-transfer-fueling-retooling April 5, 2021      !>?ȷ⥓`h_$h@r#hz~f@CJOJQJ^JaJ'h@r#h_:@CJOJQJ^JaJ h@r#h_CJOJQJ^JaJ!hEs:@CJOJQJ^JaJ)h@r#hPS5>*CJOJQJ\^JaJ)h8Ch8C5>*CJOJQJ\^JaJ h@r#hPSCJOJQJ^JaJ#h@r#hPS5CJOJQJ^JaJ h@r#hOCJOJQJ^JaJ#h@r#h8C5CJOJQJ^JaJ  `#`"|/ p0^p`0gd )^gd ) ^`gd )gd )^gdj^gd0n & Fgd  & Fgd  & Fgd  & Fgda^gdz~f ? 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