91°µÍø

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Wide-angle diamond cell for neutron scattering

Publication Type
Journal
Journal Name
High Pressure Research
Publication Date
Page Numbers
495 to 506
Volume
37
Issue
4

A new diamond cell with extreme apertures is described. It is tailored for a large variety of neutron scattering techniques such as inelastic neutron scattering and single-crystal diffraction both at the Spallation Neutron Source (SNS) and the High Flux Isotope Reactor at the 91°µÍø. Simple springs enable forces of over 10 metric tons to be clamped in for low-temperature measurements. At present, low-cost polycrystalline diamond (Versimax®) pressure anvils are used. We predict a routine pressure regime up to 20 GPa with sample volumes of ∼0.5 mm3. Future use of large CVD single-crystal diamond anvils will significantly expand this pressure range. We show examples for measurements at the SNAP, VISION and CORELLI beamlines of the SNS.